                                        INSTRUMENT CONTROL PARAMETERS:    MS3_Enh
                                        -----------------------------------------

   C:\MSDCHEM\1\DATA\2014-01-24-1555.B\SCN_DD_HP5MS_DRV.M
      Sat Jan 25 00:26:43 2014

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled


 No Sample Prep method has been assigned to this method.

Oven
Equilibration Time                           3 min
Max Temperature                              325 degrees C
Slow Fan                                     Disabled
Oven Program                                 On
    65 °C for 1 min
    then 20 °C/min to 320 °C for 6.25 min
Run Time                                     20 min
Cryo                                         Off

Front Injector
Syringe Size                                 10 ?L
Injection Volume                             1 ?L
Solvent A Washes (PreInj)                    0
Solvent A Washes (PostInj)                   5
Solvent A Volume                             8 ?L
Solvent B Washes (PreInj)                    2
Solvent B Washes (PostInj)                   2
Solvent B Volume                             8 ?L
Sample Washes                                0
Sample Wash Volume                           2 ?L
Sample Pumps                                 0
Dwell Time (PreInj)                          0 min
Dwell Time (PostInj)                         0 min
Solvent Wash Draw Speed                      300 ?L/min
Solvent Wash Dispense Speed                  1000 ?L/min
Sample Wash Draw Speed                       300 ?L/min
Sample Wash Dispense Speed                   1000 ?L/min
Injection Dispense Speed                     6000 ?L/min
Viscosity Delay                              3 sec
Sample Depth                                 -2 mm
Injection Type                               2-layer Sandwich
L1 Airgap                                    1 ?L
L2 Volume                                    0.2 ?L
L2 Airgap                                    0.4 ?L

Back Injector
Syringe Size                                 100 ?L
Injection Volume                             10 ?L
Solvent A Washes (PreInj)                    0
Solvent A Washes (PostInj)                   0
Solvent A Volume                             80 ?L
Solvent B Washes (PreInj)                    0
Solvent B Washes (PostInj)                   0
Solvent B Volume                             80 ?L
Sample Washes                                0
Sample Wash Volume                           80 ?L
Sample Pumps                                 0
Dwell Time (PreInj)                          0 min
Dwell Time (PostInj)                         0 min
Solvent Wash Draw Speed                      1000 ?L/min
Solvent Wash Dispense Speed                  3000 ?L/min
Sample Wash Draw Speed                       1000 ?L/min
Sample Wash Dispense Speed                   3000 ?L/min
Injection Dispense Speed                     3000 ?L/min
Viscosity Delay                              3 sec
Sample Depth                                 Disabled
Injection Type                               Standard
L1 Airgap                                    0 ?L

Barcode Reader
Barcode heater                               Disabled
Barcode mixer                                Disabled

Sample Overlap
Sample overlap will occur after the previous injection is completed

Front SS Inlet He
Mode                                         Pulsed Splitless
Heater                                       On    250 °C
Pressure                                     On    13.317 psi
Total Flow                                   On    54.456 mL/min
Septum Purge Flow                            On    3 mL/min
Septum Purge Flow Mode                       Switched
Gas Saver                                    On    15 mL/min After 4 min
Injection Pulse Pressure                     36.259 psi Until 0.5 min
Purge Flow to Split Vent                     50 mL/min at 1 min

Thermal Aux 2 (MSD Transfer Line)
Heater                                       On
Temperature Program                          On
    290 °C for 0 min
Run Time                                     20 min

Column #1
Agilent 19091S-433: 93.92873
HP-5MS  5% Phenyl Methyl Silox
325 °C: 30 m x 250 ?m x 0.25 ?m
In: Front SS Inlet He
Out: Vacuum

(Initial)                                    65 °C
Pressure                                     13.317 psi
Flow                                         1.4559 mL/min
Average Velocity                             44.295 cm/sec
Holdup Time                                  1.1288 min
Flow Program                                 Off
    1.4559 mL/min for 0 min
Run Time                                     20 min

Signals
Signal #1: None

Signal #2: None

Signal #3: Test Plot                         Save Off
                                             50 Hz

Signal #4: Test Plot                         Save Off
                                             50 Hz

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 3.75 min

EMV Mode                 : Gain Factor
Gain Factor              : 1.50
Resulting EM Voltage     : 2529

[Scan Parameters]

Low Mass                 : 42.0
High Mass                : 700.0
Threshold                : 150
Sample #                 : 2       A/D Samples    4
Plot 2 low mass          : 50.0
Plot 2 high mass         : 650.0

[MSZones]

MS Source                : 230 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US71216556
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      27.945
 IONFOCUS    :      90.157
 ENTRANCE_LE :      16.000
 EMVOLTS     :    1964.706
                               Actual EMV  :    2529.41
                               GAIN FACTOR :       1.50
 AMUGAIN     :    1496.000
 AMUOFFSET   :     123.625
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      20.329
 MASSGAIN    :    -930.000   
 MASSOFFSET  :     -37.000   

                           END OF TUNE PARAMETERS
                      ------------------------------------



                                           END OF INSTRUMENT CONTROL PARAMETERS
                                           ------------------------------------
