

                           INSTRUMENT CONTROL PARAMETERS:    MSD5975C
                           ------------------------------------------

   C:\MSDCHEM\1\METHODS\NARCO_HP-5MS.M
      Thu May 29 22:58:40 2014

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled

Oven
Equilibration Time                           0.5 min
Oven Program                                 On
    100 C for 3 min
    then 25 C/min to 300 C for 20 min
Run Time                                     31 min





Front Injector
Syringe Size                                 10 L
Injection Volume                             1 L
Solvent A Washes (PreInj)                    2
Solvent A Washes (PostInj)                   1
Solvent A Volume                             8 L
Solvent B Washes (PreInj)                    2
Solvent B Washes (PostInj)                   1
Solvent B Volume                             8 L
Sample Washes                                0
Sample Wash Volume                           1 L
Sample Pumps                                 2
Dwell Time (PreInj)                          0 min
Dwell Time (PostInj)                         0 min
Solvent Wash Draw Speed                      300 L/min
Solvent Wash Dispense Speed                  6000 L/min
Sample Wash Draw Speed                       300 L/min
Sample Wash Dispense Speed                   6000 L/min
Injection Dispense Speed                     6000 L/min
Viscosity Delay                              0 sec
Sample Depth                                 -1 mm
Injection Type                               Standard
L1 Airgap                                    0 L


Sample Overlap
Sample overlap is not enabled



Front SS Inlet He
Mode                                         Pulsed Splitless
Heater                                       On    280 C
Pressure                                     On    21.369 psi
Total Flow                                   On    44 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    On    20 mL/min After 2 min
Injection Pulse Pressure                     25 psi Until 0.5 min
Purge Flow to Split Vent                     40 mL/min at 0.5 min


Thermal Aux 2 {MSD Transfer Line}
Heater                                       On
Temperature Program                          On
    280 C for 0 min
Run Time                                     31 min


Column #1
DB-5ms EVDX: 1107.77781
DB-5ms EVDX
325 C: 25 m x 200 m x 0.33 m
In: Front SS Inlet He
Out: Vacuum

(Initial)                                    100 C
Pressure                                     21.369 psi
Flow                                         1 mL/min
Average Velocity                             40.853 cm/sec
Holdup Time                                  1.0199 min
Flow Program                                 On
    1 mL/min for 0 min
Run Time                                     31 min




Valve 1
Other                                        Off









Valve Box
Heater                                       Off

Signals
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz


                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : urtune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 4.00 min

EMV Mode                 : Relative
Relative Voltage         : 106
Resulting EM Voltage     : 1424

[Scan Parameters]

Low Mass                 : 40.0
High Mass                : 550.0
Threshold                : 50
Sample #                 : 2       A/D Samples    4

[MSZones]

MS Source                : 230 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US93414024
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      32.971
 IONFOCUS    :      90.157
 ENTRANCE_LE :      25.500
 EMVOLTS     :    1317.647
                               Actual EMV  :    1423.53
                               GAIN FACTOR :       0.44
 AMUGAIN     :    1924.000
 AMUOFFSET   :     122.500
 FILAMENT    :       2.000
 DCPOLARITY  :       1.000
 ENTLENSOFFS :      18.824
 MASSGAIN    :    -683.000   
 MASSOFFSET  :     -38.000   

                           END OF TUNE PARAMETERS
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                              END OF INSTRUMENT CONTROL PARAMETERS
                              ------------------------------------

