                         INSTRUMENT CONTROL PARAMETERS:    GBUZ AO BSME
                         ----------------------------------------------

   C:\MSDCHEM\1\METHODS\SKRIN_SCAN.M
      Tue May 24 11:33:14 2016

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled


 No Sample Prep method has been assigned to this method.

Oven
Equilibration Time                           1 min
Max Temperature                              300 degrees C
Slow Fan                                     Enabled
Oven Program                                 On
    60 °C for 1 min
    then 10 °C/min to 280 °C for 7 min
Run Time                                     30 min




Front Injector
Syringe Size                                 10 µL
Injection Volume                             1 µL
Solvent A Washes (PreInj)                    5
Solvent A Washes (PostInj)                   5
Solvent A Volume                             8 µL
Solvent B Washes (PreInj)                    5
Solvent B Washes (PostInj)                   5
Solvent B Volume                             8 µL
Sample Washes                                6
Sample Wash Volume                           8 µL
Sample Pumps                                 1
Dwell Time (PreInj)                          0 min
Dwell Time (PostInj)                         0 min
Solvent Wash Draw Speed                      300 µL/min
Solvent Wash Dispense Speed                  6000 µL/min
Sample Wash Draw Speed                       300 µL/min
Sample Wash Dispense Speed                   6000 µL/min
Injection Dispense Speed                     6000 µL/min
Viscosity Delay                              0 sec
Sample Depth                                 Disabled
Injection Type                               Standard
L1 Airgap                                    0.2 µL


Sample Overlap
Sample overlap is not enabled



Front SS Inlet He
Mode                                         Split
Heater                                       On    250 °C
Pressure                                     On    56.756 kPa
Total Flow                                   On    7 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    Off
Split Ratio                                  3 :1
Split Flow                                   3 mL/min


Thermal Aux 2 (MSD Transfer Line)
Heater                                       On
Temperature Program                          On
    280 °C for 0 min
Run Time                                     30 min


Column #1
Agilent 19091S-433HP-5MS  5% Phenyl Methyl Silox
325 °C: 30 m x 250 µm x 0.25 µm
In: Front SS Inlet He
Out: Vacuum

(Initial)                                    60 °C
Pressure                                     56.756 kPa
Flow                                         1 mL/min
Average Velocity                             36.623 cm/sec
Holdup Time                                  1.3653 min
Flow Program                                 On
    1 mL/min for 0 min
Run Time                                     30 min



Signals
Signal #1: None
Signal #2: None
Signal #3: None
Signal #4: None

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 3.50 min

EMV Mode                 : Absolute
Resulting EM Voltage     : 1800

[Scan Parameters]

Low Mass                 : 15.0
High Mass                : 550.0
Threshold                : 0
Sample #                 : 2       A/D Samples    4

[MSZones]

MS Source                : 230 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US11488715
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      24.092
 IONFOCUS    :      90.157
 ENTRANCE_LE :      35.000
 EMVOLTS     :    1529.412
                               Actual EMV  :    1800
                               GAIN FACTOR :       1.53
 AMUGAIN     :    2194.000
 AMUOFFSET   :     122.625
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      18.322
 MASSGAIN    :    -515.000   
 MASSOFFSET  :     -39.000   

                           END OF TUNE PARAMETERS
                      ------------------------------------



                              END OF INSTRUMENT CONTROL PARAMETERS
                              ------------------------------------
