                            INSTRUMENT CONTROL PARAMETERS:    gcms
                            --------------------------------------

   C:\MSDCHEM\1\METHODS\SCREEN.M
      Fri Oct 14 19:14:25 2016

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled


 No Sample Prep method has been assigned to this method.

=============================================================================
                                6850 GC METHOD
=============================================================================


OVEN
   Initial temp:  70 'C (On)               Maximum temp:  325 'C
   Initial time:  0.50 min                 Equilibration time:  0.50 min
   Ramps:
      #  Rate  Final temp  Final time
      1 99.00      100        1.00
      2 60.00      300       13.00
      3   0.0(Off)
   Post temp:  0 'C
   Post time:  0.00 min
   Run time:  18.14 min


INLET (SPLIT/SPLITLESS)                 DETECTOR (NO DET)
   Mode:  Splitless                        Temperature:  280 'C (On)
   Initial temp:  270 'C (On)
   Pressure:  5.65 psi (On)
   Purge flow:  25.0 mL/min
   Purge time:  0.00 min
   Total flow:  27.3 mL/min
   Gas saver:  Off
   Gas type:  Helium


COLUMN                                  SIGNAL
   Capillary Column                        Data rate:  0.1 Hz
   Model Number:  Agilent 19091S-433E      Type:  col comp
   HP-5MS  5% Phenyl Methyl Siloxane       Save Data:  Off
   Max temperature:  325 'C                Zero:  0.0 (Off)
   Nominal length:  30.0 m                 Range:  0
   Nominal diameter:  250.00 um            Fast Peaks:  Off
   Nominal film thickness:  0.25 um        Attenuation:  0
   Mode:  constant flow
   Initial flow:  0.9 mL/min
   Nominal init pressure:  7.60 psi
   Average velocity:  35 cm/sec
   Source:  Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum


COLUMN COMP
   Use:  Valve Box Heater


VALVES                                  POST RUN
                                           Post Time: 0.00 min


TIME TABLE
   Time       Specifier                     Parameter & Setpoint




                               GC Injector


     Front Injector:
        Sample Washes                 1
        Sample Pumps                  3
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       5
        PreInj Solvent B Washes       5
        PostInj Solvent A Washes      3
        PostInj Solvent B Washes      3
        Viscosity Delay               0 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.00 minutes
        PostInjection Dwell        0.00 minutes


     Back Injector:
No parameters specified

 Column 1 Inventory Number : AB002
                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 3.00 min

EMV Mode                 : Absolute
Resulting EM Voltage     : 1024

[Scan Parameters]

Low Mass                 : 45.0
High Mass                : 600.0
Threshold                : 150
Sample #                 : 2       A/D Samples    4

[MSZones]

MS Source                : 230 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US30945822
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      28.950
 IONFOCUS    :      87.310
 ENTRANCE_LE :      19.000
 EMVOLTS     :    1023.529
                               Actual EMV  :    1023.53
                               GAIN FACTOR :       0.66
 AMUGAIN     :    2568.000
 AMUOFFSET   :     135.000
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      18.824
 MASSGAIN    :     678.000   
 MASSOFFSET  :      -7.000   

                           END OF TUNE PARAMETERS
                      ------------------------------------



                             END OF INSTRUMENT CONTROL PARAMETERS
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