                INSTRUMENT CONTROL PARAMETERS:    Instrument#1
                ----------------------------------------------

   D:\MassHunter\GCMS\1\methods\Alex.M
      Wed Dec 14 20:23:22 2016

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  Manual
Mass Spectrometer :  Enabled


 No Sample Prep method has been assigned to this method.


GC
Oven
Temperature
Setpoint                                     On
(Initial)                                    90 °C
Hold Time                                    2 min
Post Run                                     115 °C
Program
#1 Rate                                      10 °C/min
#1 Value                                     260 °C
#1 Hold Time                                 6 min


Equilibration Time                           0.3 min
Max Temperature                              350 °C
Slow Fan                                     Disabled
Cryo                                         Off

Front SS Inlet He
Mode                                         Splitless
Heater                                       On    250 °C
Pressure                                     On    15.494 psi
Total Flow                                   On    14.5 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    Off
Purge Flow to Split Vent                     10 mL/min at 2 min
Liner                                        Agilent 5190-2293: 900 μL (Splitless, single taper, ultra inert )

Thermal Aux 2 (MSD Transfer Line)
Temperature
Setpoint                                     On
(Initial)                                    270 °C
Hold Time                                    0 min
Post Run                                     0 °C


Column
Column #1
Flow
Setpoint                                     On
(Initial)                                    1.5 mL/min
Hold Time                                    0 min
Post Run                                     1 mL/min

Agilent 19091S-433UI                         
HP-5ms Ultra Inert                           
0 °C—325 °C (350 °C): 30 m x 250 μm x 0.25 μm
Column lock                                  Unlocked
In                                           Front SS Inlet He
Out                                          MSD 
(Initial)                                    90 °C
Pressure                                     15.494 psi
Flow                                         1.5 mL/min
Average Velocity                             45.477 cm/sec
Holdup Time                                  1.0995 min


Aux EPC 1,2,3
Aux EPC 1 He
Pressure
Setpoint                                     Off
(Initial)                                    3.756 psi
Hold Time                                    0.5 min
Post Run                                     0 psi
Program
#1 Rate                                      0.60242 psi/min
#1 Value                                     10.834 psi
#1 Hold Time                                 1 min


                                             ***Excluded from Affecting GC's Readiness State***

Aux EPC 2 N2
Pressure
Setpoint                                     Off
(Initial)                                    10 psi
Hold Time                                    0 min
Post Run                                     0 psi

                                             ***Excluded from Affecting GC's Readiness State***

Aux EPC 3 N2
Pressure
Setpoint                                     Off
(Initial)                                    10 psi
Hold Time                                    0 min
Post Run                                     0 psi

                                             ***Excluded from Affecting GC's Readiness State***


Signals
Signal #1:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Front Sample

Signal #2:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Back Sample

Signal #3:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Back Sample

Signal #4:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Back Sample




MS Information
-- -----------


General Information
------- -----------

Acquisistion Mode        : Scan
Solvent Delay (minutes)  : 4.00
Tune file                : D:\MassHunter\GCMS\1\ATUNE.U
EM Setting mode Gain     : 1.000000

Normal or Fast Scanning  : Normal Scanning
Trace Ion Detection      : Off
Run Time (if MS only)    : 650 minutes 

[Scan Parameters]
Start Time               : 4.00
Low Mass                 : 40.00
High Mass                : 550.00
Threshold                : 150
A/D Samples:             : 4


[MSZones]

MS Source                   : 230 C   maximum 250 C
MS Quad                     : 150 C   maximum 200 C

Timed Events
----- ------
Number Events= 0



                     END OF MS ACQUISTION PARAMETERS


                        TUNE PARAMETERS for SN: US1345M210
                        ---------------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.593
 ENERGY      :      70.007
 REPELLER    :      34.899
 IONFOCUS    :      90.331
 ENTRANCE_LE :      17.627
 EMVOLTS     :    1205.823
                               Actual EMV  :    1151.1
                               GAIN FACTOR :       1.00
 AMUGAIN     :    1276.000
 AMUOFFSET   :     125.375
 FILAMENT    :       1.000
 DCPOLARITY  :       1.000
 ENTLENSOFFS :      11.317
 MASSGAIN    :    -618.000   
 MASSOFFSET  :     -37.000   

                        END OF TUNE PARAMETERS
                        ----------------------



                      END OF INSTRUMENT CONTROL PARAMETERS
                      ------------------------------------
