                    INSTRUMENT CONTROL PARAMETERS:    GC_MSD
                    ----------------------------------------

   D:\MassHunter\Methods\ivanov\DOAS.M
      Mon Jan 22 13:44:02 2018

Control Information
------- -----------

Sample Inlet             : GC
Injection Source         : GC ALS
Injection Location:  Rear
Mass Spectrometer        : Enabled


 No Sample Prep method has been assigned to this method.


GC
Oven
Temperature
Setpoint                                     On
(Initial)                                    50 °C
Hold Time                                    0.5 min
Post Run                                     100 °C
Program
#1 Rate                                      99 °C/min
#1 Value                                     100 °C
#1 Hold Time                                 1 min
#2 Rate                                      15 °C/min
#2 Value                                     280 °C
#2 Hold Time                                 30 min


Equilibration Time                           1 min
Max Temperature                              325 °C
Maximum Temperature Override                 Disabled
Slow Fan                                     Disabled
Cryo                                         Off

ALS
Back Injector
Syringe Size                                 10 μL
Injection Volume                             1 μL
Solvent A Washes (PreInj)                    4
Solvent A Washes (PostInj)                   0
Solvent A Volume                             8 μL
Solvent B Washes (PreInj)                    4
Solvent B Washes (PostInj)                   4
Solvent B Volume                             8 μL
Sample Washes                                1
Sample Wash Volume                           8 μL
Sample Pumps                                 5
Dwell Time (PreInj)                          0 min
Dwell Time (PostInj)                         0 min
Solvent Wash Draw Speed                      300 μL/min
Solvent Wash Dispense Speed                  3000 μL/min
Sample Wash Draw Speed                       300 μL/min
Sample Wash Dispense Speed                   3000 μL/min
Injection Dispense Speed                     6000 μL/min
Viscosity Delay                              0 sec
Sample Depth                                 Disabled
Injection Type                               Standard
L1 Airgap                                    0.2 μL
Solvent Wash Mode                            A, B

Sample Overlap
Mode                                         Sample overlap is not enabled

ALS Errors                                   Pause for user interaction

Front MM Inlet He
Temperature
Setpoint                                     Off
(Initial)                                    250 °C
Post Run                                     250 °C

Mode                                         Splitless
Heater                                       Off
Pressure                                     Off
Total Flow                                   Off
Septum Purge Flow                            Off
Purge Flow to Split Vent                     15 mL/min at 0.35 min
Cryo                                         Off

Back SS Inlet He
Mode                                         Split
Heater                                       On    270 °C
Pressure                                     On    10 psi
Total Flow                                   On    10.327 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    Off
Split Ratio                                  5 :1
Split Flow                                   6.1057 mL/min
Liner                                        Agilent 5190-3162: 900 μL (Splitless, single taper, ultra inert )

Thermal Aux 2 (MSD Transfer Line)
Temperature
Setpoint                                     On
(Initial)                                    280 °C
Post Run                                     0 °C


Column
Column #1
Pressure
Setpoint                                     On
(Initial)                                    10 psi
Post Run                                     10.523 psi

Agilent 19091S-433UI                         
HP-5ms Ultra Inert                           
0 °C—325 °C (350 °C): 30 m x 250 μm x 0.25 μm
Column lock                                  Unlocked
In                                           Back SS Inlet He
Out                                          MSD 
(Initial)                                    50 °C
Pressure                                     10 psi
Flow                                         1.2211 mL/min
Average Velocity                             40.273 cm/sec
Holdup Time                                  1.2415 min

Column Outlet Pressure                       0 psi

Aux EPC 1,2,3
Aux EPC 1 N2
Pressure
Setpoint                                     Off
(Initial)                                    10 psi
Post Run                                     0 psi

                                             ***Excluded from Affecting GC's Readiness State***

Aux EPC 2 N2
Pressure
Setpoint                                     Off
(Initial)                                    10 psi
Post Run                                     0 psi

                                             ***Excluded from Affecting GC's Readiness State***

Aux EPC 3 N2
Pressure
Setpoint                                     Off
(Initial)                                    10 psi
Post Run                                     0 psi

                                             ***Excluded from Affecting GC's Readiness State***


Signals
Signal #1:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Front Sample

Signal #2:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Back Sample

Signal #3:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Back Sample

Signal #4:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Back Sample




MS Information
-- -----------


General Information
------- -----------

Acquisition Mode         : Scan
Solvent Delay (minutes)  : 3
Tune file                : D:\MassHunter\GCMS\1\5977\atune.u
EM Setting mode Gain     : 1.000000

Normal or Fast Scanning  : Normal Scanning
Trace Ion Detection      : Off
Run Time (if MS only)    : 650 minutes 

[Scan Parameters]
Start Time               : 3
Low Mass                 : 41
High Mass                : 650
Threshold                : 150
A/D Samples:             : 4


[MSZones]

MS Source                   : 230 C   maximum 250 C
MS Quad                     : 150 C   maximum 200 C

Timed Events
----- ------
Number Events= 0



                     END OF MS ACQUISTION PARAMETERS


                        TUNE PARAMETERS for SN: US1515M415
                        ---------------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.593
 ENERGY      :      70.007
 REPELLER    :      34.899
 IONFOCUS    :      90.331
 ENTRANCE_LE :      15.136
 EMVOLTS     :    1176.708
                               Actual EMV :  1162.2
                               GAIN FACTOR :   1.00
 AMUGAIN     :    1070.000
 AMUOFFSET   :     123.750
 FILAMENT    :       1.000
 DCPOLARITY  :       1.000
 ENTLENSOFFS :      13.566
 Ion_Body    :       0.000
 EXTLENS     :       0.005
 MASSGAIN    :    -682.000   
 MASSOFFSET  :     -35.000   

                        END OF TUNE PARAMETERS
                        ----------------------



                      END OF INSTRUMENT CONTROL PARAMETERS
                      ------------------------------------
