

                              INSTRUMENT CONTROL PARAMETERS
                              -----------------------------

=============================================================================
                               6890 GC METHOD
=============================================================================

OVEN
   Initial temp:  50 'C (On)               Maximum temp:  450 'C
   Initial time:  0.00 min                 Equilibration time:  0.00 min
   Ramps:
      #  Rate  Final temp  Final time
      1 20.00      320        2.00
      2   0.0(Off)
   Post temp:  50 'C
   Post time:  0.00 min
   Run time:  15.50 min

FRONT INLET (SPLIT/SPLITLESS)           BACK INLET (UNKNOWN)
   Mode:  Splitless
   Initial temp:  265 'C (On)
   Pressure:  7.88 psi (On)
   Purge flow:  1.0 mL/min
   Purge time:  0.00 min
   Total flow:  5.2 mL/min
   Gas saver:  On
   Saver flow:  20.0 mL/min
   Saver time:  3.00 min
   Gas type:  Helium

COLUMN 1                                COLUMN 2
   Capillary Column                        (not installed)
   Model Number:  HP 19091J-433
   HP-5  5% Phenyl Methyl Siloxane
   Max temperature:  325 'C
   Nominal length:  30.0 m
   Nominal diameter:  250.00 um
   Nominal film thickness:  0.25 um
   Mode:  constant flow
   Initial flow:  1.0 mL/min
   Nominal init pressure:  7.89 psi
   Average velocity:  37 cm/sec
   Inlet:  Front Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum

FRONT DETECTOR ()                       BACK DETECTOR ()
   Temperature:  250 'C (Off)              Temperature:  250 'C (Off)
    flow:  40.0 mL/min (Off)               Mode:  Constant makeup flow
    flow:  450.0 mL/min (Off)              Makeup flow:  60.0 mL/min (Off)
   Mode:  Constant makeup flow             Makeup Gas Type: Nitrogen
    flow:  45.0 mL/min (Off)               Electrometer:  Off
   Makeup Gas Type: Nitrogen
   Flame:  Off
   Electrometer:  Off
   Lit offset:  2.0

SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  test plot                        Type:  test plot
   Save Data:  On                          Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0

COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)

THERMAL AUX 2
   Use:  MSD Transfer Line Heater
   Description:
   Initial temp:  300 'C (On)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)

                                        POST RUN
                                           Post Time: 0.00 min

TIME TABLE
   Time       Specifier                     Parameter & Setpoint


                              7673 Injector


     Front Injector:
        Sample Washes                 5
        Sample Pumps                  5
        Injection Volume            1.0 microliters
        Syringe Size               10.0 microliters
        PostInj Solvent A Washes      4
        PostInj Solvent B Washes      4
        Viscosity Delay               0 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.00 minutes
        PostInjection Dwell        0.00 minutes

     Back Injector:
No parameters specified

 Column 1 Inventory Number :  
 Column 2 Inventory Number :  

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 3.00 min

EM Absolute              : True
Resulting EM Voltage     : 1623.5

[Scan Parameters]

Low Mass                 : 40.0
High Mass                : 620.0
Threshold                : 0
Sample #                 : 3       A/D Samples    8
Plot 2 low mass          : 271.8
Plot 2 high mass         : 272.1

[MSZones]

MS Quad                  : 150 C   maximum 200 C
MS Source                : 230 C   maximum 250 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS
                        -----------------------------

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      25.097
 IONFOCUS    :      90.157
 ENTRANCE_LE :      23.000
 EMVOLTS     :    1717.647
 AMUGAIN     :    2210.000
 AMUOFFSET   :     126.000
 FILAMENT    :       1.000
 DCPOLARITY  :       1.000
 ENTLENSOFFS :      18.573
MASSGAIN     :     -71.929   
MASSOFFSET   :     -10.048   


                           END OF TUNE PARAMETERS
                      ------------------------------------





                           END OF INSTRUMENT CONTROL PARAMETERS
                           ------------------------------------

