

                                     INSTRUMENT CONTROL PARAMETERS:    Instrument #1
                                     -----------------------------------------------

   C:\MSDCHEM\1\METHODS\SCR_evidex_2010.M

Control Information
------- -----------
       Sample Inlet : GC
   Injection Source : GC/ALS
 Injection Location : ALS
             Use MS : Yes

=============================================================================
                                6850 GC METHOD
=============================================================================

OVEN
   Initial temp:  130 'C (On)              Maximum temp:  350 'C
   Initial time:  5.00 min                 Equilibration time:  1.00 min
   Ramps:
      #  Rate  Final temp  Final time
      1 10.00      320        5.00
      2   0.0(Off)
   Post temp:  0 'C
   Post time:  0.00 min
   Run time:  29.00 min

INLET (SPLIT/SPLITLESS)                 DETECTOR (NO DET)
   Mode:  Splitless                        Temperature:  250 'C (On)
   Initial temp:  280 'C (On)
   Pressure:  23.37 psi (On)
   Purge flow:  20.0 mL/min
   Purge time:  2.00 min
   Total flow:  22.5 mL/min
   Gas saver:  Off
   Gas type:  Helium

COLUMN                                  SIGNAL
   Capillary Column                        Data rate:  50 Hz
   Model Number:  Agilent 100-2000         Type:  col comp
   DB-5MSEVDX                              Save Data:  Off
   Max temperature:  325 'C                Zero:  0.0 (Off)
   Nominal length:  25.0 m                 Range:  0
   Nominal diameter:  200.00 um            Fast Peaks:  Off
   Nominal film thickness:  0.33 um        Attenuation:  0
   Mode:  constant flow
   Initial flow:  1.0 mL/min
   Nominal init pressure:  23.38 psi
   Average velocity:  41 cm/sec
   Source:  Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum

COLUMN COMP
   Use:  Valve Box Heater

VALVES                                  POST RUN
                                           Post Time: 0.00 min

TIME TABLE
   Time       Specifier                     Parameter & Setpoint


                               GC Injector


     Front Injector:
        Sample Washes                 1
        Sample Pumps                  6
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       2
        PreInj Solvent B Washes       0
        PostInj Solvent A Washes      1
        PostInj Solvent B Washes      0
        Viscosity Delay               0 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.00 minutes
        PostInjection Dwell        0.00 minutes

     Back Injector:
No parameters specified

 Column 1 Inventory Number : AB001
                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 5.00 min

EM Absolute              : False
EM Offset                : 200
Resulting EM Voltage     : 1494.1

[Scan Parameters]

Low Mass                 : 70.0
High Mass                : 400.0
Threshold                : 150
Sample #                 : 2       A/D Samples    4
Plot 2 low mass          : 50.0
Plot 2 high mass         : 550.0

[MSZones]

MS Quad                  : 150 C   maximum 200 C
MS Source                : 230 C   maximum 250 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN:  
                        -----------------------------

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      34.814
 IONFOCUS    :      90.157
 ENTRANCE_LE :      12.000
 EMVOLTS     :    1294.118
 AMUGAIN     :    2569.000
 AMUOFFSET   :     133.000
 FILAMENT    :       1.000
 DCPOLARITY  :       1.000
 ENTLENSOFFS :      20.329
 MASSGAIN    :     701.000   
 MASSOFFSET  :      -7.000   


                           END OF TUNE PARAMETERS
                      ------------------------------------



                                           END OF INSTRUMENT CONTROL PARAMETERS
                                           ------------------------------------

