

                  INSTRUMENT CONTROL PARAMETERS:    US 90411863
                  ---------------------------------------------

   C:\MSDCHEM\1\METHODS\SPACE.M
      Mon Jun 27 08:48:22 2011

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  Manual
Mass Spectrometer :  Enabled

=============================================================================
                                6850 GC METHOD
=============================================================================


OVEN
   Initial temp:  100 'C (On)              Maximum temp:  300 'C
   Initial time:  2.00 min                 Equilibration time:  0.50 min
   Ramps:
      #  Rate  Final temp  Final time
      1 20.00      290       15.00
      2   0.0(Off)
   Post temp:  290 'C
   Post time:  5.00 min
   Run time:  26.50 min


INLET (SPLIT/SPLITLESS)                 DETECTOR (NO DET)
   Mode:  Split                            Temperature:  280 'C (On)
   Initial temp:  280 'C (On)
   Pressure:  10.47 psi (On)
   Split ratio:  30:1
   Split flow:  29.9 mL/min
   Total flow:  33.7 mL/min
   Gas saver:  On
   Saver flow:  15.0 mL/min
   Saver time:  2.00 min
   Gas type:  Helium


COLUMN                                  SIGNAL
   Capillary Column                        Data rate:  0.1 Hz
   Model Number:  Agilent 19091S-433E      Type:  col comp
   HP-5MS  5% Phenyl Methyl Siloxane       Save Data:  Off
   Max temperature:  325 'C                Zero:  0.0 (Off)
   Nominal length:  30.0 m                 Range:  0
   Nominal diameter:  250.00 um            Fast Peaks:  Off
   Nominal film thickness:  0.25 um        Attenuation:  0
   Mode:  constant flow
   Initial flow:  1.0 mL/min
   Nominal init pressure:  10.47 psi
   Average velocity:  37 cm/sec
   Source:  Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum


COLUMN COMP
   Use:  Valve Box Heater


VALVES                                  POST RUN
                                           Post Time: 5.00 min
                                           Oven Temperature: 290 'C
                                           Column 1 Flow: 1.0 mL/min


TIME TABLE
   Time       Specifier                     Parameter & Setpoint




                               GC Injector


     Front Injector:
No parameters specified

     Back Injector:
No parameters specified

 Column 1 Inventory Number : AB001
                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 2.50 min

EMV Mode                 : Relative
Relative Voltage         : 0
Resulting EM Voltage     : 1259

[Scan Parameters]

Low Mass                 : 40.0
High Mass                : 550.0
Threshold                : 150
Sample #                 : 2       A/D Samples    4

[MSZones]

MS Source                : 230 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US90411863
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      25.600
 IONFOCUS    :      80.667
 ENTRANCE_LE :      19.000
 EMVOLTS     :    1258.824
                               Actual EMV  :    1258.82
                               GAIN FACTOR :       0.23
 AMUGAIN     :    1447.000
 AMUOFFSET   :     126.063
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      18.071
 MASSGAIN    :    -866.000   
 MASSOFFSET  :     -36.000   

                           END OF TUNE PARAMETERS
                      ------------------------------------



                      END OF INSTRUMENT CONTROL PARAMETERS
                      ------------------------------------

